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Organic Synteses vol 69 - Paquette L.A.

Paquette L.A., Boecman R.K. Organic Synteses vol 69 - John Wiley & Sons, 1990. - 174 p.
ISBN 0-471-54560-0
Download (direct link): organicsynthesesvol691990.pdf
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(E)-1-Hexenyl-1,3,2-benzodioxaborole: 1,3,2-Benzodioxaborole, 2-(1-hexenyl)-, (E)-;
37490-22-5), 68, 130 (E)-I-Hexenyldiisobutylalane; (20259-40-9), 66, 66 (E)-1 -Hexenyl iodide; (16644-98-7), 66, 63, 66 (Z)-1 -Hexenyl iodide; (16538-47-9), 66, 61, 62, 66 3-Hexylcyclobutanone, 69, 199
1-Hexyne; (693-02-7), 66, 66; 68, 32, 130
reaction with diisobutylaluminum hydride, 66, 63 Higher order cuprates, 66, 57
HOFMANN REARRANGEMENT UNDER MILDLY ACIDIC CONDITIONS, 66, 132
Homoenolate, copper, 66, 47
Homoenolate, titanium, 66, 47
HOMOENOLATE, ZINC, 66, 43
Horner-Wadsworth-Emmons reaction, 66, 220
Hydrazine, 66, 143; 67, 60, 187
Hydrazine, tert-butyl, monohydrochloride, 65, 166
Hydrazine, (1,1-dimethylethyl)-, monohydrochloride, 65, 166
Hydroalumination of alkynes, 66, 64
Hydroboration of alkynes, 66, 64
of 1 -alkyne with catecholborane, 68, 130 Hydrocinnamoyl chloride: Benzenepropanoyl chloride; (645-45-4), 69, 180 Hydrogen; (1333-74-0), 68, 64,182, 228 Hydrogenation, homogeneous, directed, 68, 64 Hydrogen chloride, 66, 144, 146 Hydrogenolysis, 68, 227
Hydrogen peroxide; (7722-84-1), 65, 166; 68, 83, 130, 162; 69, 97 Hydrogen sulfide, 66,143, 145
293
Hydroperoxide, 1-methyl-1-phenylethyl; (80-15-9), 68, 49 Hydroquinone: 1,4-Benzenediol; (123-31-9), 67, 98 as diene stabilizer, 66, 63 3-HYDROXY-1 -CVCLOHEXENE-1 -CARBOXALDEHYDE: 1-CYCLOHEXENE-1 -CARBOXALDEHYDE, 3-HYDROXY-; (67252-14-6), 67, 205 (S)-(+)-3-HYDROXY-2,2-DIMETHYLCYCLOHEXANONE: Cyclohexanone, 3-hydroxy-
2,2-dimethyl-, (S)-; (87655-21-8), 68, 56 Hydroxylamine, N-phenyl-, 67, 187 a-Hydroxylation of ketones, 66, 138
1 -(HYDROXYMETHYL)CYCLOHEXANOL: CYCLOHEXANEMETHANOL,
1-HYDROXY-; (15753-47-6), 69, 96
1-HYDROXYMETHYL-4-(1-METHYLCYCLOPROPYL)-1-CYCLOHEXENE:
1-CYCLOHEXENE-1-METHANOL, 4-(1-METHYLCYCLOPROPYL)-;
(536-59-4), 67, 176
3-HYDROXY-3-METHYL-1-PHENYL-1-BUTANONE: 1-BUTANONE,
3-HYDROXY-3-METHYL-1 -PHENYL-; (43108-74-3), 65, 6, 12
1-(3-HYDROXY-2-METHYL-3-PHENYLPROPANOYL)PIPERIDINE, ERYTHRO: PIPERIDINE, 1 -(3-HYDROXY-2-METHYL-1 -OXO-3-PHENYLPROPYL)-, R*,R*)-(±)-; (99114-36-0), 69, 44 N-Hydroxymethylphthalimide: Phthalimide, N-(hydroxymethyl)-;
1H-lsoindole-1,3-(2H)-dione, 2-(hydroxymethyl)-; (118-29-6), 65, 119
3-HYDROXY-2-NITROCYCLOHEXYL ACETATE, (1S,2S,3R): 1,3-
CYCLOHEXANEDIOL, 2-NITRO-, 1-ACETATE, [1S-(1a,2ß,3a)]-;
(108186-61-4), 69, 19
3-Hydroxy-1-nonene: 1-Nonen-3-ol; (21964-44-3), 68, 210 (2S*,3S*)-3-HYDROXY-3-PHENYL-2-METHYLPROPANOIC ACID, 68, 83 (1-Hydroxy-2-propenyl)trimethylsilane, 66, 14,15
294
3-HYDROXY-2,2,3-TRIMETHYLOCTAN-4-ONE: 4-OCTANONE, 3-HYDROXY-2,2,3,-TRIMETHYL-; (85083-71-2), 69, 114 Hydrozirconation of alkynes, 66, 64 Hypervalent iodine compounds, 66, 138
Imines, reduction by diisobutylaluminum hydride, 66, 189 5H-lnden-5-one, 1,2,3,3a,4,6-hexahydro-, 67, 163 INDOLE, 4-NITRO-, 65, 146
INTRAMOLECULAR ACYLATION OF ALKYLSILANES, 66, 87 INVERSE ELECTRON DEMAND DIELS-ALDER, 65, 98 Iodine; (7553-50-2), 68, 198 Iodine, hypervalent, 68, 175
Iodine, phenylbis(trifluoroacetato-O); (2712-78-9), 66,141 lodobenzene diacetate, 66, 136 lodobenzene dichloride, 66, 137
6-lodo-3,4-dimethoxybenzaldehyde cyctohexylimine: Cyclohexanamine, N-[(2-iodo-4,5-dimethoxyphenyl)methylene]-; (61599-78-8), 65, 108 lodomethane; (74-88-4), 68, 56, 116,162
lodosobenzene diacetate: Benzene, (diacetoxyiodo)-; (3240-34-4), 68,175
0-lodotoluene; (615-37-2), 66, 67, 68, 74
1-lodo-3-trimethylsilylpropane; (18135-48-3), 66, 87, 88, 91, 94 Ion exchange chromatography, 66. 212, 214, 215
Iron pentacarbonyl, 66, 99 Isobutene; (115-11-7), 67, 52 Isobutyl chloride, 69, 107 Isobutyl chloroformate, 66, 135 Isobutylmagnesium chloride, 69, 106
295
(R)-lsobutyloxirane, 66, 165
lsoindole-1,3-(2H)-dione, 2-(bromomethyl)-, 1H-, 65, 119 lsoindole-1,3-(2H)-dione, 2-(hydroxymethyl)-, 1H-, 65, 119 (S)-lsoleucine, 66, 153
Isomenthol, (+)-: Cyclohexanol, 5-methyl-2-(1-methylethyl)-, [1S-(1a,2(3,5p)];
(23283-97-8), 65, 81 Isomenthone, (+)-: Cyclohexanone, 5-methyl-2-(1 -methylethyl)-, (2R-cis)-;
(1196-31-2), 65, 81 ISOPRENE; (78-79-5), 67, 48
(Isopropoxydimethylsilyl)methyl chloride: Silane, (chloromethyl)isopropoxydimethyl-;
(18171-11-4), 69, 96
1-[(lsopropoxydimethylsilyl)methyl]cyclohexanol, 69, 96 Isopropyl alcohol, titanium (4+) salts; (546-68-9), 65, 230; 67,180; 68, 49 Isopropylideneacetophenone: 2-Buten-1-one, 3-methyl-1-phenyl-;
(5650-07-7), 65, 12 Isopropylidene a-(hexahydroazepinylidene-2)malonate: 1,3-Dioxane-4,6-
dione, 5-(hexahydro-2H-azepin-2-ylidene)-2,2-dimethyl-; (70192-54-8),
67, 170 (R)-lsopropyloxirane, 66, 165
Isoquinoline, 1,2,3,4-tetrahydro-6,7-dimethoxy, hydrochloride, 67,60 Isoquinoline, 1,2,3,4-tetrahydro-6,7-dimethoxy-1-methyl-, (S)-, 67, 60
Jones' reagent, 68, 175
Ketones, preparation from carboxylic acid, 66, 119
296
ß-Lactams, 65, 140
Lactic acid, 2-methyl-, methyl ester; (2110-78-3), 66,114 Lead dioxide: Lead oxide; (1309-60-0), 65, 166 Lead oxide, 65, 166 Lead tetraacetate; (546-67-8), 69, 190 (S)-Leucine, 66, 153
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