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Organic Synteses vol 69 - Paquette L.A.

Paquette L.A., Boecman R.K. Organic Synteses vol 69 - John Wiley & Sons, 1990. - 174 p.
ISBN 0-471-54560-0
Download (direct link): organicsynthesesvol691990.pdf
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a,ß-Acetylenic esters from ß-chloroalkylidene malonates, 66, 178
3-ACETYL-4-HYDROXY-5,5-DIMETHYLFURAN-2(5H)-ONE, 66, 108, 110 N-ACETYL-N-PHENYLHYDROXYLAMINE: ACETOHYDROXAMIC ACID, N-
PHENYL; ACETAMIDE, N-HYDROXYL-N-PHENYL-; (1795-83-1), 67, 187 ACETYLTRIMETHYLSILANE: Silane, acetyltrimethyl; (13411-48-8), 68, 25
4-ACRIDINOL, 9-BUTYL-1,2,3,4,5,6,7,8-OCTAHYDRO; (99922-91-5), 69, 226 Acrylonitrile; 2-Propenenitrile; (107-13-1), 65, 236
256
Acyl chlorides, preparation, 66, 116 Acylsilanes, preparation, 66, 18
ADDITION OF TIN RADICALS TO TRIPLE BONDS, 66, 75 Adipic acid monomethyl ester; (627-91-8), 66, 116, 117, 120 Alane, (E)-l-decenyldiisobutyl-, 66, 60, 61 (S)-Alanine (L-alanine); (56-41-7), 66, 151-153, 159 Alanine, phenyl-, L-; (63-91-2), 68, 77 Aldehydes, preparation from carboxylic acid, 66, 124 Aldol reaction, 65, 6, 12
diastereoselective, 68, 83 Alkenylzinc reagents, 66, 64 Alkylation, of ester enolate, 66, 87 (R)-Alkyloxiranes, properties, 66,169
(R)-ALKYLOXIRANES OF HIGH ENANTIOMERIC PURITY, 66, 160
ALKYNE ISOMERIZATION. 66,127
Aliéné; (463-49-0), 69, 121
Aliéné, 1-methyl-1-(trimethylsilyl)-, 66, 8, 9
Aliénés, synthesis by Claisen rearrangement, 66, 22
(3—Allenic esters, conjugation by alumina, 66, 26
ALLENYLSILANES, SYNTHESIS OF, 66, 1
Ally! alcohol; (107-18-6), 66, 14, 16, 21
Allyl bromide; (106-95-6), 68, 104; 69, 57
ALLYLCARBAMATES, 65, 159
Allyl ester enolate (Carroll) rearrangement, 68, 210
Allylic acétoxylation, 68, 109
Allylmagnesium bromide; (1730-25-2), 68, 104
(E)-3-Allyloxyacrylic acids, 66, 33, 34
257
ALLYLTRIBUTYLTIN: Stannane, tributyl-2-propenyl-; (24850-33-7), 68, 104
Allyl trimethylsilyl ether, metallation, 66, 18
Aluminate(l-), dihydrobis-2-(methoxyethanalato)-, sodium, 67, 13
Aiuminate(l-), tetrahydro-, lithium, 67, 69
Aluminum chloride, 66, 90
Aluminum oxide, 66, 23
Aluminum, hydrobis(2-methylpropyl)-; (1191-15-7), 66, 193
Aluminum, triisobutyl, 67, 176
Aluminum, tripropyl-; (102-67-0), 66, 193
Amberlite IR-120 (plus), acid form; (78922-04-0), 69, 21
Amberlyst 15 ion exchange resin, 66, 203, 206; 69, 159
Amino acids, determination of enantiomeric purity, 66, 153
1-AMINO-2-METHOXYMETHYLPYRROLIDINE, (R)-(+)- (RAMP), 65, 173
1-AMINO-2-METHOXYMETHYLPYRROLIDINE, (S)-(-)- (SAMP), 65, 173, 183
2-Amino-1-phenyl-1,3-propanediol, (1S,2S)-(+)-: 1,3-Propanediol, 2-amino-1-phenyl; (3306-06-7), 69, 55
3-Aminopropylamine: 1,3-Propanediamine; (109-76-2), 65, 224 Ammonia, 66, 133, 135
Ammonium acetate; (631-61-8), 69, 228 Ammonium, benzyltrimethyl-, hydroxide; (100-85-6), 68, 56 Anisole, 2,4-dichloro-, 67, 222 [3+3] Annulation, 66, 4, 8, 10, 11
a-D-Arabino-Hexopyranose, 2-deoxy, tetraacetate; (16750-06-4), 69, 66 Asymmetric alkylation, 67, 60 Asymmetric synthesis, 65,183, 215
of cycloalkane dicarboxylates, 67, 76 AZA-ENE REACTION, 65, 159
258
1H-Azepine, hexahydro-2-propyl-; (85028-29-1), 66, 193 2H-Azepine, 3,4,5,6-tetrahydro-7-methoxy-, 67, 170 2-AZETIDINONE, 4-(ACETYLOXY)-, 65, 135 2-AZETIDINONE, 4-HYDROXY-ACETATE (ESTER), 65, 135
2-AZETIDINONE, 3-METHOXY-1.3-DIMETHYL-4-PHENYL-, 65, 140 Azobisisobutyronitrile (AIBN); (78-67-1), 66, 77, 79, 86; 67, 86; 69, 66 AZOMETHINE YLIDE EQUIVALENT, 67, 133
1 (2H)-AZULENONE-3,4-DIHYDRO: 1(2H)-AZULENONE, 3,4-DIHYDRO-; (52487-41-9), 69, 180
Beckmann rearrangement, 66, 185, 189, 190 Benzaldehyde; (100-52-7), 65, 119; 66, 203; 68, 83 Benzaldehyde, 2-bromo-4,5-dimethoxy-, 65, 108 Benzaldehyde, 3-nitro-, 67, 180 Benzene, (2-bromoethenyl)- (Z)-; (588-73-8), 68, 130 Benzene, (1-cyclopenten-1-ylsulfonyl)-, 67, 157, 163 Benzene, 2,4-dichloro-1-methoxy-, 67, 222 Benzene, 1-(ethynylsulfonyl)-4-methyl-, 67, 149 Benzene, 1-methyl-4-(methylthio)-; (623-13-2), 68, 49 BENZENE, [(NITROMETHYL)THIO]-; (60595-16-6), 68, 8 Benzeneamine, N-hydroxy-, 67, 187 Benzeneamine, 2-methyl-3-nitro-, 65,146
1,2-Benzenediol; (120-80-9), 66, 184; 67, 98
Benzenemethanamine, N-(methoxymethyl)-N-[(trimethylsilyl)methyl]-, 67, 133 Benzenemethanamine, N-[(trimethylsilyl)methyl]-, 67, 133 Benzenemethanaminium, N,N,N-trimethyl-, hydroxide; (100-85-6), 68, 56 Benzenemethanol, a-methyl-3-nitro-, 67, 180
259
Benzenemethanethiol, 65, 215 Benzenepropanol, 2-amino-, (S)-; (3182-95-4), 68, 77 Benzeneseleninic acid, 67, 157 Benzenesulfenyl chloride; (931-59-9); 68, 8 Benzenesulfonamide, 66, 203 Benzenesulfonic acid, hydrazide, 67, 157 Benzenesulfonoselenoic acid, Se-phenyl ester, 67, 157
1-(BENZENESULFONYL)CYCLOPENTENE: BENZENE, (1 -CYCLOPENTEN-1 -YLSULFONYL)-; (64740-90-5), 67, 157, 163 Benzenesulfonyl hydrazide: Benzenesulfonic acid, hydrazide; (80-17-1), 67, 157 Benzenethiol; (108-98-5), 68, 8
2H-1-BENZOPYRAN, 3.4-DIHYDRO-2-METHYLENE; (74104-13-5), 69, 72 2H-1 -BENZOPYRAN-3-CARBOXYLIC ACID, 5,6,7,8-TETRAHYDRO-2-OXO-,
METHYL ESTER, 65, 98 p-Benzoquinone; (106-51-4), 67, 105; 68, 109; 69, 38 4H-1,3-BENZOXATHIIN, HEXAHYDRO-4,4,7-TRIMETHYL-, 65, 215 Benzoyl chloride; (98-88-4), 69, 45 Benzoyl chloride, 4-nitro-, 67, 86
1 -(2-Benzoylpropanoyl)piperidine: Piperidine, 1 -(2-methyl-1,3-dioxo-3-phenylpropyl)-, (±)-; (99114-34-8), 69, 44 Benzyl alcohol, a-methyl-m-nitro-, 67, 180 Benzylamine; (100-46-9), 67, 105, 133; 68, 227 Benzylamine hydrochloride; (3287-99-8), 68, 206
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