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Organic Synteses vol 69 - Paquette L.A.

Paquette L.A., Boecman R.K. Organic Synteses vol 69 - John Wiley & Sons, 1990. - 174 p.
ISBN 0-471-54560-0
Download (direct link): organicsynthesesvol691990.pdf
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H.; Knutson, P. L. Org. Synth. 1986, 64, 144.
29. Tietze, L. F.; Br├╝ggemann, K. Angew. Chem., Intern. Ed. Eng. 1982, 21, 539.
30. Tietze, L. F.; Bergmann, A.; Br├╝ggemann, K. Synthesis 1986, 190.
243
31. Tietze, L. F.; Bergmann, A. Angew. Chem., Intern. Ed. Engl. 1985, 24, 127.
32. Tietze, L. F.; Voss, E.; Harms, K.; Sheldrick, G. M. Tetrahedron Lett. 1985, 26, 5273.
Appendix Chemical Abstracts Nomenclature (Collective Index Number); (Registry Number)
Ethyl 3,3-diethoxypropanoate: Propanoic acid, 3,3-diethoxy-, ethyl ester (9); (10601-80-6).
1,1,1-Trichloro-4-ethoxy-3-buten-2-one: 3-Buten-2-one, 1,1,1-trichloro-4-ethoxy- (11); (83124-74-7)
Trichloroacetyl chloride: Acetyl chloride, trichloro- (8,9); (76-02-8)
Ethyl vinyl ether: Ether, ethyl vinyl (8); Ethene, ethoxy- (9); (109-92-2)
Methyl 3,3-dimethoxypropanoate: Propanoic acid, 3,3-dimethoxy-, methyl ester (9); (7424-91-1)
Methyl vinyl ether: Ether, methyl vinyl (8); Ethene, methoxy- (9); (107-25-5)
1,1,1 -Trichloro-4-methoxy-3-buten-2-one: 3-Buten-2-one, 1,1,1 -trichloro-4-methoxy-, (E)- (12); (116140-91-1)
244
Unchecked Procedures
Accepted for checking during the period May 1,1989 through June 1,1990. An asterisk (*) indicates that the procedure has been subsequently checked.
In accordance with a policy adopted by the Board of Editors, beginning with Volume 50 and further modified subsequently, procedures received by the Secretary and subsequently accepted for checking will be made available upon request to the Secretary, if the request is accompanied by a stamped, self-addressed envelope. (Most manuscripts require 540 postage).
Address requests to:
Professor Jeremiah P. Freeman Organic Syntheses, Inc.
Department of Chemistry University of Notre Dame Notre Dame, Indiana 46556
It should be emphasized that the procedures which are being made available are unedited and have been reproduced just as they were first received from the submitters. There is no assurance that the procedures listed here will ultimately check in the form available, and some of them may be rejected for publication in Organic Syntheses during or after the checking process. For this reason, Organic Syntheses can provide no assurance whatsoever that the procedures will work as described and offers no comment as to what safety hazards may be involved. Consequently, more than usual caution should be employed in following the directions in the procedures.
Organic Syntheses welcomes, on a strictly voluntary basis, comments from persons who attempt to carry out the procedures. For this purpose, a Checker's Report form will be mailed out with each unchecked procedure ordered. Procedures which have been checked by or under the supervision of a member of the Board of Editors will continue to be published in the volumes of Organic Syntheses, as in the past. It is anticipated that many of the procedures in the list will be published (often in revised form) in Organic Syntheses in future volumes.
245
2509R
2527
2539*
2541*
2542*
2545*
2546*
2547
2548*
2549*
2553*
Preparation and Diels-Alder Reaction of a Reactive, Electron-Deficient Heterocyclic Azadiene: Dimethyl l,2,4,5-Tetrazine-3,6-Dicarboxylate. 1,2-Diazine and Pyrrole Introduction.
D. L. Boger, J. S. Panek, and M. Patel, Department of Chemistry, Purdue University, West Lafayette, IN 47907
(-)-(lS,4R)-Camphanoyl Chloride.
D. Kappes and H. Gerlach, Laboratorium fur Organische Chemie, Universit├Ąt Bayreuth, Postfach 101251, D-8580 Bayreuth,
West Germany
2-Phenyl-2,3,4,5-Tetramethylphosphole.
P. J. Fagan and W. A. Nugent, E. I. du Pont de Nemours & Co., Inc. Central Research & Development Department, Experimental Station, Wilmington, DE 19898
Synthesis of Furans via Rhodium(II) Acetate Catalyzed Reaction of Acetylenes with a-Diazocarbonyls.
H. M. L. Davies, W. R. Cantrell, Jr., and J. S. Baum, Department of Chemistry, Wake Forest University, Winston-Salem, NC 27109
Nickel-Catalyzed Silylolefination of Allylic Dithioacetals: (E,E)-Trimethyl(4-Phenyl-1,3-butadienyl)si lane.
Z.-J. Ni and T.-Y. Luh, Department of Chemistry, The Chinese University of Hong Kong, Shatin, N.T., Hong Kong
a-Acetylenic Esters from a-Acylmethylenephosphoranes: Ethyl 4,4,4-Trifluorotetrolate.
B. C. Hamper, Monsanto Agricultural Co., 800 N. Lindburgh Blvd.,
St. Louis, M0 63167
4-Benzyl-10,19-diethyl-4,10,19-triaza-l ,7,13,16-tetraoxacycloheneicosane (Triaza-21-crown-7).
K. E. Krakowiak and J. S. Bradshaw, Department of Chemistry, Brigham Young University, Provo, UT 84602
Methoxycarbonylmethylation of Aldehydes via Siloxycyclopropanes: Methyl 3,3-Dimethyl-4-oxobutanoate.
H.-U. Reissig, I. Reichelt, and T. Kunz, Institut fur Organishe Chemie, Technische Hochschule Darmstadt, 6100 Darmstadt,
Petersenstr. 22, Federal Republic of Germany
Tetrahydro-3-benzazepin-2-ones: Lead Tetraacetate Oxidation of Isoquinoline Enamides.
G. R. Lenz and R. A. Lessor, Health Care R & D, The B0C Group, Inc., 100 Mountain Ave., Murry Hill, NJ 07974
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