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Organic Synteses vol 70 - Meyers A.I.

Meyers A.I. , Boecman R.K. Organic Synteses vol 70 - John Wiley & Sons, 1992. - 163 p.
ISBN 0-471-57743
Download (direct link): organicsynthesesvol701992.pdf
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1.2.4.5-Tetrazine-3,6-dicarboxylic acid, 1,2-dihydro-, disodium salt; (96898-32-7), 70, 80
s-Tetrazine-3,6-dicarboxylic acid, dimethyl ester; (2166-14-5), 70, 79
2-Thiaadamantane, 70, 126
(endo,endo)-9-Thiabicyclo[3.3.1]nonane-2,6-diol, 70, 121
9-Thiabicyclo[3.3.1]nonane-2,6-diol, (endo.endo)-; (22333-35-3), 70, 121
9-THIABICYCLO[3.3.1]NONANE-2,6-DIONE; (37918-35-7), 70, 120
2-Thiabrexane, 70, 126
Thiacycloheptane, 70, 126
Thiacyclohexane, 70, 126
Thionyl chloride; (7719-09-7), 70, 80, 130
Thiophenes, 70, 276
Thymine polyoxin, 70, 27
p-Toluenesulfonic acid, 70, 71
p-Toluenesulfonic acid monohydrate; (6192-52-5), 70, 13, 19, 217, 233
Toluenesulfonyl azide, 70, 97
Transition metal carbene complexes, 70, 186
Triaza-21-crown-7, 70, 132
Tributylstannane, 70, 166
Trichloromethyl chloroformate, 70, 72
Trifluoroacetic acid; (76-05-1), 70, 11, 141
304
Trifluoroacetic anhydride, 70, 246
(E,E)-TRIMETHYL(4-PHENYL-1,3-BUTADIENYL)SILANE, 70, 240
1-Trimethylsilyl-1-hexyne, 70, 215 (Trimethylsilyl)methylmagnesium chloride, 70, 241 Trimethylsilyl trifluoromethanesulfonate, 70, 101, 234 Triphenylphosphine, 70, 1, 248
Triphenyiphosphine: Phosphine, triphenyl-; (603-35-0), 70, 10 Trisilane, 1,1,1,3,3,3-hexamethyl-2-(trimethylsilyl)-; (1873-77-4), 70, 164 TRIS(TRIMETHYLSILYL)SILANE, 70, 164
Urea, N-methyl-N-nitroso-; (684-93-5), 70, 22
L-Vinylglycine hydrochloride, 70, 30
Zinc; (7440-66-6), 70, 195 Zinc bromide; (7699-45-8), 70, 55, 157 Zinc-copper couple, 70, 186 Zinc dust, 70, 85
Zirconium, dichloro-71-cyclopentadienyl-, 70, 272 Zirconium metallacycle, 70, 274 Zirconocene dichloride, 70, 272
305
ORGANIC
SYNTHESES
AN ANNUAL PUBLICATION OF SATISFACTORY METHODS FOR THE PREPARATION OF ORGANIC CHEMICALS
Volume 70 1992
BOARD OF EDITORS
Albert I. Meyers, Editor-in-Chief Robert K. Boeckman, Jr. Amos B. Smith III
David L. Coffen James D. White
Larry E. Overman Ekkehard Winterfeldt
Leo A. Paquette Hisashi Yamamoto
Ichiro Shinkai
Theodora W. Greene, Assistant Editor Jeremiah P. Freeman, Secretary to the Board Department of Chemistry, University of Notre Dame,
Notre Dame, Indiana 46556
Richard T. Arnold Henry E. Baumgarten Richarde. Benson Virgil Boekelheide Ronald Bkeslow Arnold Brossi George H. Büchi T. J. Cairns James Cason Orville L. Chapman Robert M. Coates E. J. Corey William G. Dauben William D. Emmons
ADVISORY BOARD
Albert Eschenmoser Ian Fleming Clayton H. Heathcock E. C. Horning Herbert O. House Robert E. Ireland Carl R. Johnson William S. Johnson Andrew S. Kende N. J. Leondard
B. C. McKusick Satoru Masamune Wataru Nagata Melvin S. Newman
Wayland E. Noland Ryoji Noyori Charles C. Price Norman Rabjohn John D. Roberts Gabriel Saucy Dieter Seebach Martin F. Semmelhack Ralph L. Shriner Bruce E. Smart H. R. Snyder Edwin Vedeis Kenneth B. Wibero Petf.r Yates
FORMER MEMBERS OF THE BOARD,
Roger Adams Homer Adkins C. F. H. Allen Werner E. Bachmann A. H. Blatt Wallace H. Carothers H. T. Clarke J. B. Conant Arthur C. Cope
NOW DECEASED
Nathan L. Drake L. F. Fieser R. C. Fuson Henry Gilman CliffS. Hamilton W. W. Hartman John R. Johnson Oliver Kamm C. S. Marvel
C. R. Noller W. E. Parham R. S. Schreiber John C. Sheehan William A. Sheppard Lee Irvin Smith Robert V. Stevens Max Tishler Frank C. Whitmore
JOHN WILEY & SONS, INC.
New York • Chichester • Brisbane • Toronto • Singapore
Published by John Wiley & Sons, Inc.
Copyright © 1992 by Organic Syntheses, Inc.
All rights reserved. Published simultaneously in Canada.
Reproduction or transiation of any part of this work beyond that permitted by Section 107 or 108 of the 1976 United States Copyright Act without the permission of the copyright owner is unlawful.
“John Wiley & Sons, Inc. is pleased to publish this volume of Organic Syntheses on behalf of Organic Syntheses, Inc. Although Organic Syntheses, Inc. has assured us that each preparation contained in this volume has been checked in an independent laboratory and that any hazards that were uncovered are clearly set forth in the write-up of each preparation, John Wiley & Sons, Inc. does not warrant the preparations against a.ny safety hazards and assumes no liability with respect to the use of the preparations.’’
Library of Congress Catalog Card Number: 21-17747 ISBN 0-471 -57743-X
Printed in the llniicd States of America
10 () H 7 *> 4 \ 2 I
NOTICE
With Volume 62, the Editors of Organic Syntheses began a new presentation and distribution policy to shorten the time between submission and appearance of an accepted procedure. The soft cover edition of this volume is produced by a rapid and inexpensive process, and is sent at no charge to members of the Organic Divisions of the American and French Chemical Society, The Perkin Division of the Royal Society of Chemistry, and The Society of Synthetic Organic Chemistry, Japan. The soft cover edition is intended as the personal copy of the owner and is not for library use. A hard cover edition is published by John Wiley and Sons Inc. in the traditional format, and differs in content primarily in the inclusion of an index. The hard cover edition is intended primarily for library collections and is available for purchase through the publisher. Annual Volumes 60-64 have been incorporated into a new five-year version of the collective volumes of Organic Syntheses which has appeared as Collective Volume Seven in the traditional hard cover format. It is available for purchase from the publishers. The Editors hope that the new Collective Volume series, appearing twice as frequently as the previous decennial volumes, will provide a permanent and timely edition of the procedures for personal and institutional libraries. The Editors welcome comments and suggestions from users concerning the new editions.
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