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Sulfur reagents in organic - Metzner P.

Metzner P., Thuiller A. Sulfur reagents in organic - Academic press, 1994. - 200 p.
Download (direct link): sulfarreagents1994.djvu
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I
Index
A
Acyl silanes 17 Aldol reaction of dithioesters 106 of imidothiolesters 117 of thiolesters 113 Alkenes
from Chugaev reaction 53 from Julia reaction 129 from Ramberg-Backlund reaction 128 from vicinal dixanthates 58 synthesis from sulfoximines 134 via Kocienski method 129 via two-fold extrusion 138 Alkenyl sulfides
in [4+2] cycloaddition 166 reaction with Grignard reagents 94.146 synthesis from ketones 91 synthesis from thiolesters 137 Alkenyl sulfoxides in [4+2] cycloadditon 166 Allylic amination 160 Amino esters syriihesis uf 82 trans (+)-a-Atlantone 116

Bakers yeast reduction uf p-uxudilhkolcrs 102 Barton deoxygenation reaction 46,59,60
1,2- enzen e di t hiol 3
2-(Benzenesulfonyl)tetrahydro-2H-pyran
132
Bis(dimethylalummium) 1,3-propanedithioloate 20
l.l-Bis(methylthio)-l,3-butadiene 22 Bis(methy]thio)dihydrofurans 146 Bis(phenyhhio)methyllithium 87 Bis(trimethylsilyl)peroxide 72 Bis(trimethylsilyl)sulfide 31 (?)-l,3-Butadienyl(tributyl)stannane 177 Butenolides 121 ()-2-(l-tert-Butyl-2,2-
dimethylpropylidene)bomene 164

Carbon disulfide 19,21,33,40,47 110 Cheletropic reactions 172 Cholestane 61
Cholestanol thionocarbonate 61 Chugaev reaction 46.53 Claisen rearrangement 154 Claycop reagent 14 Clayfen reagent 14 Corey-Winter alkene synthesis 58 Crown sulfdes 8 [4+2] Cycloaddition 164 Cyclohexenyl cyclohexyl methanol 92 2-3(3-Cyclohexenylidene)-l ,3-dithiane 21 Cyclohexenyllithium 92 Cyclolpentyl propyl ketone 79 Cyclopropanation with Helquist reagent 149 with sulfones 150 with sulfur ylides 147,149,153
D
DAST 70 Davis reagents 27
Davy reagents 32,38 decarboxylation 64,67 Dehydrogenation of ketones 55 Dehydrohalogenation 57 Deracemization 68 Desulfurization 75 of dithioacetals 78,100 of dithioesters 69
of sulfides 81.85,95,104,118,122,146 of sulfones 123,125 of thiiranes 53.139,141 Di-t-butyl ketone imine 33 D-t-butyl thioketone 34 DIBAH 121
Diels-Alder reaction (see also [4+2] Cycloaddition) of thioaldehydes 31 of vinuylsulfonium salts 168
1.3-Dienes
from sulfolenes 173 ,V,/V-Diethylthioacetamide 45
2.6-Dimethylheptane-4-thione 35 Dimethyl trisulfide 12 Dimethylphenylthioaluminum 20 (lR,5/?)-6.6-Dimethyl-3-
(phenylthio)bicyclo[3.1.1 ]hept-3-en-2-one 66
Diols
in alkene synthesis 58
1.7-Dioxal[5.5]undecane 132 Diphenyl disulfide 54 Dipolar cycloadditions 163 Disodium trithicarbonate 57 Disulfides
synthesis of 11 3.6-Diethyl-J,5-octadiene 174 Dithiane oxides alkylation of 84 carbanions of 84 Dithianes alkylation of 76,79 as acyl anion equivalents 75 carbanions of 76,79 cleavage of 14-18.76,79 desulfurization of 78 oxidation of 23
1.3-Dithiane-l. dioxide 24
1.3-Dithiane-l-oxide 24 Dithioacetal dioxides
alkylation of 83 cleavage of 83 Dithioacetal monoxides alkylation of 103 carbanions of 81-84,103 cleavage of 81-84 synthesis of 81-84 Dithioacetals (see also dithianes and dithiolanes) alkylation of 98 as acyl anion equivalents 75 carbanions of 87,97-102 cleavage of 14-18,98,102 desulfurization of 78 metal-catalysed coupling 127 reaction with Grignard reagents 127 reductive lithiation of 89 synthesis of 12-19,97-102 Dithioacids synthesis of 40 Dithiocarbonates see xanthates Dithioesters aldol reaction of 106 as acyl anion equivalents 106 carbophilic addition with Grignard reagents 100 carbophilic addition with lithiocuprates
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