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Organic Synthess - McKusick B.C.

McKusick B.C., Boekelheide V., Emmons W.D. Organic Synthess - New York, 1963. - 134 p.
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2-Nitro-2,3-dimethylbutane, 43, 89
1-Nitro-l,4-dimethylcyclohexene, 43, 89
2-Nitro-2,4-dimethylpentane, 43, 89 2-Nitroethanot., 41, 67
conversion to nitroethylene, 41, 71 Nitroethylene, 41,71
2-Nitrofluorene, reduction to 2-amino-fluorene, 40, 5 Nitrogen, purification of, 41, 97 Nitromethane in condensation with formaldehyde, 41, 67
1-Nitro-l-methylcyclohexane, 43, 89
1-Nitro-l-methylcyclopentane, 43, 89
2-Nitro-2-methylpropane, 43, 89 N-Niteomoreholine, 43, 83 0-Nitroperoxybenzoic acid, 43, 96 p-Nitrophenacylamine, hydrochloride
of, 41, 87 m-NlTROPHENYL DISULFIDE, 40, 80 />-Nitrophenyl isocyanide, 41, 103 Nitrosation of o-acetotoluidide by oxides of nitrogen, 42, 69 N-Nitroso-N-methyl-N'-nitroguanidine, diazomethane from, 41, 10 Niteosomethylueethane, warning because a carcinogen, 43, 86
o-Nitrotoluene, condensation with ethyl oxalate, 43, 40
4-Nitro-2,2,4-teimethylpentane, 43, 87
SUBJECT INDEX
119
Nitrous acid in oxidation of 1,2,4-tri-azole-3(5)-thiol to 1,2,4-triazole,
40, 100
2-Norbornanone, 42, 79
2-eiee-Norborneol, 42, 81
2-eza-Norbornyl formate, 42, 79 Noecampi-ior, 42, 79 Norcarane, 41, 72
OCTADECANEDIOIC ACID, DIMETHYL ESTER, 41, 33 Octane, 2,7-dimethyl-2,7-dinitro-, 41, 24
2-Oxa-7,7-dichloronorcahane, 41, 76 Oxalyl chloride, condensation, with N,N-diethylaniline, 41, 3 with N,N-dimethylaniline, 41, 1 with NjN-di-K-propylaniiine, 41,
3
Oxidation, of acids to peroxy acids by hydrogen peroxide, 43, 96 of alkylarenes to aromatic carboxylic acids, 43, 80 of ^-aminoacetanilide to 4,4'-diamino-azobenzene by sodium perborate,
40, 18
of aryl iodides, to iodosoarene diacetates, 43, 62 to iodoxyarenes, 43, 66 of tert-buty] alcohol to a,a,a',a'-tetra-methyltetramethylene glycol by hydrogen peroxide and ferrous sulfate, 40, 90 of fert-butylamine to ce,<*,<*',a'-tetra-methyltetramethylenediamine by hydrogen peroxide and ferrous sulfate, 40, 92 of l-chloro-2,3,3-trifluorocyclobutene by permanganate, 42, 45 of Crystal Violet with hydrogen peroxide, 41, 2, 3-4 of cycloheptatriene to tropylium fluo-borate, 43, 101 of dihydroxycyclopentene mixture by chromium trioxide, 42, 36 of diisobutylene to neopentyl alcohol by hydrogen peroxide, 40, 76
Oxidation, of Grignard reagents with peresters, 41, 91; 43, 55 of 2-hydroxy-3-methylbenzoic acid to
2-hydroxyisophthalic acid by lead dioxide, 40, 48 of indene, 41, 53
of methyl disulfide to methanesulfmyl chloride by chlorine, 40, 62 of 2-ето-погогпу1 formate by chromic acid, 42, 79 of pivalic acid to ajajor^a'-tetrameth-yladipic acid by hydrogen peroxide and ferrous sulfate, 40, 92 of pivalonitrile to a,a,c/,a'-tetrameth-yladiponitrile by hydrogen peroxide and ferrous sulfate, 40,92 of trialkylmethylamines to trialkyl-nitromethanes, 43,87 of l,2,4-triazole-3(5)-thiol to 1,2,4-triazole by nitric acid, 40, 100 Oxidative decarboxylation, potassium ferricyanide in, 40, 86 OxiNDOLE, 3-ACETYL-, 40, 1 Ozone, reaction with phenanthrene, 41, 41,46
Ozonolysis, methanol as solvent for, 41,
41, 46
of phenanthrene, 41, 41, 46
Palladized charcoal in reduction of 2-ni-trofluorene to 2-aminofluorene,
40, 5
[2.21PARACYCL0PHANE, 42, S3 Paraformaldehyde, condensation with nitromethane, 41, 67
2.3.4.5.6-Penta-O-acetyl-d-gluconic acid, 41, 79
conversion to acid chloride, 41, 80
2.3.4.5.6-T'y.NTA-0-ACF,TYI.-D-GI,UCONYT. CHLORIDE, 41, 79
1,2,3,4,5-Pentachloro-5-ethylcyclo-pentadiene, 43, 90 Pentacyanopropene, 41,100 acid strength of, 41, 100 Pentane, 2,2,4-trimethyl-4-nixro, 43, 87
2,4-Pentanedione, 3-methyl-, 42, 75 Pentatricontanedioic acid, 43,39
120
SUBJECT INDEX
Peracetic acid, for oxidation of iodo-benzene to iodosobenzene diacetate, 43, 62 for oxidation of iodobenzene to iodoxybenzene, 43, 65 iodometric analysis of, 43, 63 Performic acid, reaction with indene, 41, 53
Peroxides, test for, 41, 92
Peroxy acids from carboxylic acids and 70% hydrogen peroxide, 43, 96 Peroxybenzoic acid, 43,93 iodometric analysis of, 43, 94 Peroxystearic acid, 43,96 Phf.nacvt.amt\tf. hydrochloride, 41, 82
Phenanthrene, ozonization of, 41, 41,
46
Phenylacetic acid, 43, 82 alkylation of disodium salt of, 40,
39
L-Phenylalanine, reaction with phthalic anhydride to yield N-phthalyl-L-phenylalanine, 40, 82 Phenyl (ert-BUTYL ether, 41, 91 a-Phenylethylamine, N-chlorination of,
41, 82
conversion to phenacylamine hydrochloride, 41, 82 a-Phenylethyl chloride, alkylation of sodium sodiophenylacetate with, 40,40
Phenyl isocyanate, conversion to di-phenylcarbodiimide, 43,31 Phenyl isocyanide, 41,103 Phenyllithium, reaction with allyltri-phenyltin, 41, 30 standardization of, 41, 32 Phenylmagnesium bromide, 41, 91 reaction with (ert-butyl perbenzoate,
41, 91
N-Phenylmaleimide, 41, 93 f-Phenylphenacylamine, hydrochloride of, 41, 87
N-Phenylpiperidine from sodium ben-zenesulfonate and piperidine, 40,
75
Phenylpropiolic acid, 42, 99
Phenylpyruvic acids by hydrolysis of phenylhydantoins, 43, 49 1 -Phenyl-2-thiobiuret, 42, 87
l-Phenyl-2-thio-4-ethylisobiuret, 42, 89 1 I’hcny ^ tbio l metbyHsobiuret,42,
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