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Organic Synthess - McKusick B.C.

McKusick B.C., Boekelheide V., Emmons W.D. Organic Synthess - New York, 1963. - 134 p.
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Dimethylbenzylamine, dehydrobromination of bromohexadienes with,
41, 50
2,7-Dimethyl-2,7-dinitrooctane, 41, 24
SUBJECT INDEX
113
2.3-Dimethylheptanoic add, 41, 63 4,6-Dimethyl-1-hepten-4-ol, 41, 30
2.5-Dimethyl-3-hexyne-2,5-diol, conversion to 2,2,5,5-tetramethyltetra-hydro-3-ketofuran, 40, 88
Dimethyl /3-ketoadipate, 42,44 Dimethyl 3-methylenecyclobutane-
1.2-dicarboxylate, 43, 27 pyrolysis to methyl butadienoate, 43,
71
2.3-Dimethylnaphthalene, oxidation to
2.3-naphthalenedicarboxylic acids, 43, 80
Dimethyl octadecanedioate, 41, 33
2.6-Dimethylphenyl isocyanide, 41, 103
2.2-DlMETHYL-l-PROPANOL, 40, 76 N,N-Dimethyl-l,2,2-trichlorovinyl-
amines, 41, 23
2.4-Dinitrochlorobenzene, reaction with sodium iodide to yield 2,4-di-nitroiodobenzene, 40, 34
1.3-Dinitro-4,6-dichlorobenzene, from nitration of m-dichlorobenzene,
40, 96
reaction with ammonia to yield 1,3-dmitro-4,6-diaminobenzene, 40, 97
2.4-Dinitroiodobenzene, 40, 34
1,8-Dinitro-^-menthane, 43, 89
1.6-Dioxo-8a-METHYL-l,2,3,4,6,7,8,8a-OCTAHYDRONAPHTHALENE, 41, 38
Diphenaldehyde, 41, 41 Diphenaldehydic acid, 41, 46 methyl ester of, 41, 47 Diphenic acid, 41, 47
1.4-Diphenyl-1,3-butadiene, 40, 36 Diphenylcarbodiimide, 43, 31 a,jS-DlPHENYLPROPIONIC ACID, 40, 38 Dipotassium 1,8-naphthalenedicarbox-
ylate, conversion to 2,6-naphtha-lenedicarboxylic acid, 40, 71 N,N-Di-n-propylaniline, condensation with oxalyl chloride, 41, 3 Disodium 7,16-diketodocosanedioate,
43, 3S
DlSULFIDE, BIS-(m-NITROPHENYL), 40,
80
Docosanedioic АСШ, 43, 34
5-Dodecyl-l,2,3,4,5-pentachlorocyclo-pentadiene, 43, 92
Eicosanedioic acid, 43, 39 Electrolysis, Kolbe synthesis, of 2,7-dimethyl-2,7-dinitrooctane, 41, 24
of dimethyl octadecanedioate, 41,
33
two-compartment cell for, 41, 25, 29
Elimination of hydrogen bromide from bromohexadienes with dimethyl-benzylamine, 41, 50 Enamines, 41, 65 uses of, 41, 66 Esterification, of cyanoacetic acid, 41,
5
of gluconolactone, 41, 79 of tetraacetylgluconic acid, 41, 80 of a-/S-unsaturated acids, 41, 62 preparation of sec-butyl crotonate by,
41, 60
Ethanol, 2-nitko-, 41, 67 conversion to nitroethylene, 41, 71
Ether, ^/'/-butyl phenyl, 41, 91 Etherification of cholestanol, with diazo-methane, 41, 9
3-Ethoxy-2-cyclohexenone, 40, 41 reduction to 2-cyclohexenone, 40,
14
2-(2-Ethoxyethoxy)ethanol in preparation of diazomethane, 41, 16 Ethyl a-acetyl-/3-(2,3-dimethoxy-
phenyl) propionate, cyclization to ethyl 6,7-dimethoxy-3-methyl-indenc-2-carboxylate by phosphoric acid, 40, 43 N-Ethylation of amines by ethylene, 43,
45
Ethyl carbamate, reaction with hydrox-ylamine to form hydroxyurea,
40, 60
Ethyl crotonate, 3-methylheptanoic acid from, 41, 63 Ethyl di-j.'-butylaminc, 43, 47
114
SUBJECT INDEX
Ethyl 6,7-dimethoxy-3-methylin-dene-2-carboxylate, 40, 43 Ethylene, addition to piperidine, 43, 45 5,5'-Ethylene-l,2-bis-(2-furyl)-ethane,
42, 86
5,5'-Ethylcne-l,2-bis-(2-thienyl)-e thane, 42, 86 Ethylene carbonate, reaction with potassium thiocyanate, 42, 59 Ethylene sulfide, 42, 59 Ethyl formate, reaction with cyclo-hexylamine, 41, 14 Ethyl-M-hexylamine, 43,47
5-(2-Ethylhexyl)-l,2,3,4,5-pentachloro-cyclopentadiene, 43, 92 Ethylhydrazinium hydrogen oxalate,
43, 2
Ethyl indole-2-carboxylate, 43,40 Ethyl isocyanide, 41, 15 N-Ethyi-N-methylaniline, 43,47 Ethyl o-nitrophenylpyruvate, potassium salt of, 43, 40 N-Ethylmperidine, 43,45 Ethyl-o-toluidine, 43, 47 Ethyl trichloroacetate for generation of dichlorocarbene, 41, 76
Ferrocene, reaction with bis(dimethyl-amino) methane to yield di-methylaminomethylferrocene,
40, 31
Ferrocenylacetonitrile, 40, 45 Fluoboric acid as catalyst for diazo-methane etherifications, 41, 9, 10 9-Fluorenone, 2,4,5,7-tetranitro-,
42, 95
2-Fluokenylamine, 40, 5 Formaldehyde, reaction with diethyl malonate to form diethyl bis-(hydroxymethyl)malonate, 40,27 Formamide, condensation with 4,4-dimethoxy-2-butanone to give
4-methylpyrimidine, 43, 77 Formic add, and hydrogen peroxide, with indene, 41, 53 in conversion of thiosemicarbazide to
l-formyl-3-thiosemicarbazide, 40, 99
Formic acid, in preparation of e-tolyl-formamide, 41,102
1-Formyl-3-thiosemicarbazide, conversion to l,2,4-triazole-3(5)-thiol, 40,100
Furan, reaction with bromine and methanol to yield 2,5-dimethoxy-2,5-dihydrofuran, 40, 29 Furan, 2,5-dihydro-2,5-dimethoxy-,
40, 29
2-Furanacrylomtrile, 40, 46 3(2)-Furanone, 4,5-dihydro-2,2,5j5-
TETRAMETHYL-, 40, 88 Furfural in preparation of 3-(2-furyl)-acrylonitrile, 40, 47
3-(2-Furyl)acrylonitrile, 40, 46
Gluconic acid, pentaacetyl-, d-, 41,
79
D-Glucono-5-lactone, acetylation of, 41,
80
Gluconyl chloride, pentaacetyl-, D-,
41, 79
Glycinonitrix.e, N,N-dimethyl-2-PHENYL-, 43, 25 Grignard reaction, addition of allyl-magnesium bromide to acrolein, 41,'49
1,4-addition of Grignard reagents to sec-butyl esters of a,|8-unsatu-rated acids, 41, 60-64 of arylmagnesium halides with tert-butyl perbenzoate to give aryl tert-butyl ethers, 41, 91; 43, 55 Guanidine nitrate, warning against synthesis from ammonium nitrate, 43, 48
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