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Organic Synthess - McKusick B.C.

McKusick B.C., Boekelheide V., Emmons W.D. Organic Synthess - New York, 1963. - 134 p.
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Carboxylic acids, conversion to 1,1,1-trifluoro compounds, 41, 104, 106
from enamines, 43, 39 Chlorination, nuclear, aluminum chloride as catalyst for, 40, 9 of anthracene by cupric chloride, 43, 15
of pyruvic acid by sulfuryl chloride,
40, 54
on nitrogen of amines, 41, 82 with tert-butyl hypochlorite, 41, 82 Chlorine in oxidation of methyl disulfide to methanesulfiny] chloride, 40, 62
3-Chloroacetophenone, 40,10 9-Chloroanthracene, 43, IS
3-ChlorobenzaIdehyde, 40,10 ^-Chlorobenzonitrile, 43, 59
2-ChIoro-6-methylphenyl isocyanide,
41,103
J-Chlorophenacylamine, hydrochloride of, 41, 87
0-Chlorophenyl isocyanide, 41,103 />-Chlor:>pher.yl isocyanide, 41,103
1-Chloropyrene, 43, 16 Chloropyruvic acid, 40, 54
2 -Chloro-1,1,4,4-te trafluorobu tadiene, 43, 21
1-Chloro-1,4,4-trifluorobutadiene, 43, IT
1-Chloro-2,3,3-trifluorocyclobutene, 42, 45
2-Chloro-2,3,3-trifluorocyclobutyl acetate from chlorotrifluoroethylene and vinyl acetate, 43,17
Chlorotrifluoroethylene, addition to vinyl acetate, 43, 17 reaction with aqueous sodium cyanide to form 3-chloro-2,2,3-trifluoro-propionic acid, 40, 11
l-Chloro-l,4,4-trifluoro-2-phenylbuta-diene, 43, 21
3-Chloro-2,2,3-trifluoropropionamide as by-product in synthesis of 3-chloro-2,2,3-trifluoropropionic acid, 40,12
3-Chloro-2,2,3-trifi.uoropropionic ACID, 40, 11 Cholestane, 3/S-methoXV-, 41, 9 Cholestanol, etherincation of, 41, 9 Cholestanyl methyl ether, 41, 9 Cinnamaldehyde, reaction with Wittig reagent, 40, 86 Cinnamic acid, «-(/3-hydroxystyryl)-, 'y-LACTONE, 43, 3 Condensation, of benzaldehyde with
3-benzoylpropionic acid to give a-benzylidene-7-phenyl-A®’7 -butenolide, 43, 3 of carbon dioxide and sodium methyl-acetylide, 42, 97 of cydohexanone and morpholine, 41, 65
of cyclohexene with methylene iodide,
41,72
of cyclohexylamine with ethyl formate, 41, 14 of diacetyl monoxime and 3-methyl-pentane-2,4-dione, 42,93 of diethylamine with trichloroacetyl chloride, 41, 21 of dihydropyran and ethyl trichloro-acetate, 41, 76 of 4,4-dimethoxy-2-butanone with formamide to give 4-methylpy-rimidine, 43, 77 of ethyl oxalate with o-nitrotoluene to give potassium salt of ethyl
o-nitrophenylpyruvate, 43, 40 of formaldehyde and nitromethane,
41, 67
of #-hydroxybenzaldehyde with hy-dantoin to give 5-(/>-hydroxy-benzal)hydantoin, 43, 49 of malonitrile with tetracyanoethyl-ene, 41, 99 of 2 - methyl -1,3 - cyclohexanedione with methyl vinyl ketone, 41,
38
110
SUBJECT INDEX
Condensation, of oxalyl chloride, with di-tt-alkylamlines, 41, 3 with dimethylaniline, 41, 1 of 1,1,3,3-tetraethoxypropane with thiourea to give 2-mercaptopy-rimidine, 43, 68 Coupling of ^-aminoacetanilide to 4,4'-bis(acetamido)azobenzene using sodium perborate and boric acid,
40,19
Crotonic acid, esterification with sec-butyl alcohol, 41, 60 Crystal Violet, from condensation of oxalyl chloride with dimethyl-anffine, 41, 2-4 oxidative removal of traces by hydrogen peroxide, 41, 2, 3 4 Cupric chloride as chlorinating agent, 43, 15
Cuprous B-butylmercaptide, 42,22 Cuprous chloride as catalyst for 1,4 addition of Grignard reagents to a,/?-unsaturated esters, 41, 63 CYANOACETIC ACID, /ert-BUTYL ESTER,
41, S
Cyanoacetic acid, condensation with furfural to yield 3-(2-furyl)acry-lonitrile, 40, 46 with phosphorus pentachloride, 41, 5 Cyanoacetyl chloride, 41, 5 2-Cyano-4,6-dimethylpyridine, 42, S3
1-Cyanoisoquinoline, 42,33
2-Cyano-6-methylpyridine, 42,30 2-Cyanopyridine, 42,33
4-Cyanopyridine, 42,33
2-Cyanoquinoline, 42,31 Cyclization, of o-acetoaeetochloroanilide
to 3-acetyloxindole, 40, 1 polyphosphoric acid in, 40, 43 Cycloaddition, of allenes to alkenes to form methylenecyclobutanes, 43,
30
of 1,1-dichloroethylene to chlorotri-fluoroethylene, 42, 45 of fluoroethylenes to alkenes to give cyclobutanes, 43, 21 Cycloheptatriene, oxidation to tropy-lium fluoborate, 43, 101
Cycloheptatrienocarbonium fluoborate, 43, 101
2,5-Cyclohexadiene-I-carboxylic ACID, 43, 22 Cyclohexane, methylene-, 40, 66 Cyclohexanecarboxylic acid, 3,4,5-TXIACETOXY42, 62 Cyclohexanecarboxylic acid, 3,4,5-TRIOL, 42, 62
1,3-Cyclohexakedione, 2-methyl-, 41, 56
Cyclohexanone, 2-allyl-, 42,14 Cyclohexanone, condensation with mor-pholine, 41, 65 in preparation of methylene cyclo-hexane, 40, 66 Cyclohexanone diallyl acetal, 42,
34
rearrangement to 2-allylcyclohex-anone, 42, 14 Cyclohexene, purification of, 41, 74 reaction with zinc-copper couple and methylene iodide, 41, 73 2-Cyclohexenone, 40,14 Cyclohexvlamine, reaction with ethyl formate, 41, 14 N-Cyclohexylformamide, 41,14
dehydration with phosphorus oxy-chloride, 41, 13 Cyclohexyl isocyanide, 41,13 Cydopentadiene, conversion to sodium salt, 41, 96 preparation from dimer, 41, 97; 42, SO Cyclopentadiene, 1,2,3,4,5-penta-chloro-5-ethyl-, 43, 90 Cyclopentenediol, 42, SO
2-CycIopentene-l,4-diol, 42, SI
3-Cyclopentene-l,2-diol, 42, SI 2-Cyclopentene-1,4-dione, 42, 36 2-Cyclopentene-1-one, 42, 38
2-Cyclopentenone, 42, 38 Cyclopropane, bromo-, 43, 9 Cyclopropanecarboxylic acid, conversion to bromocyclopropane, 43, 9
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