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Organic Synthess - McKusick B.C.

McKusick B.C., Boekelheide V., Emmons W.D. Organic Synthess - New York, 1963. - 134 p.
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1,4-diphenyl-l,3-butadiene,40,36 Benzene, o-bis(butylthio)-, 42,22 Benzene, I-bromo-2-fhjoro-, 43, 12 Benzene, l-iODO-2,4-DiNrrKO-, 40, 34 Benzene, iodoso, 43, 60 Benzene, iodoso-, diacetate, 43, 62 c-Benzenemthiol, 42, 54 Benzenehexol, 42, 66
1,2,4-Benzenetriamine, 5-nitro-, 40,
96
Benzhydryl chloride, alkylation of sodium sodiophenylacetate with,
40, 39
Benzil, 4,4'-bis(diethylamino)-, 41, 3 Benzil, 4,4'-B1S(dIMETHYLAM1N0)-, 41,
1
Benzil, 4,4'-bis(di-«-propylamino)-, 41,3 Benzoic acid, conversion to peroxybenzoic acid, 43, 93 reduction to 1,4-dihydrobenzoic acid, 43, 22
Benzoic acid, dithio-, carboxymethyl ESTER, 42, 100 Benzopyrazole, 42, 69 3-Benzoylpropionic acid, condensation with benzaldehyde to give a-benzylidene-T-phenyl-A*3, '>'-bu-tenolide, 43, 3
N-Benzylacetamide, 42, IS n-Benzylacrylamide, 42,16 Benzyl alcohol, reaction with acryloni-trile, 42,16
a-BENZYT,IDENE-y-PHENYE-Ae'1'-BtJ-
TENOLIDE, 43, 3 Benzyl isocyanide, 41, 14
1-Benzylpiperazine, 42,19 Bicyclo[4.1.0]heptane, 41, 72 Biphenyl, 2,2'-diformyl-, 41, 41
2-Biphenylcarboxylic acid, 2'-FORMYL-, 41, 46
methyl ester of, 41, 47 Birch reduction of benzoic acid, 43, 22
1.2-Bis(b-butylthio)benzene, 42,22
1.4-Bis(«-butylthio)benzene, 42,24 4,4'-Bis(diethylamino)benzil, 41, 3 4,4'-Bis(dimethylamino)benzil, 41, 1 Bis(dimethylammo)methane, reaction
with ferrocene to yield dimethyl-aminomethylferrocene, 40, 31 4,4'-Bis(di-re-propylamino)benzil, 41, 3 Bis-(N-methyl-N-nitroso)terephthal-
amide, preparation of diazometh-ane from, 41, 16
1.4-Bis-(4-phenylbutadienyl)benzene,
40, 86
1.2-Bis(phenylthio)benzene, 42,24
1.4-Bis(phenylthio)benzene, 42, 24 £-Bis(trifluoromethyl)benzene, 41, 106
2.4-Bis(trifluoromethyl)chlorobenzene, 41,106
BlDRET, 1-PHENYL-2-THIO-, 42, 87 Bromination, nuclear, aluminum chloride as catalyst for, 40, 7 of cyclopropanecarboxylic acid to bromocvclopropane, 43, 9 of phthalide using N-bromosuccin-imide, 42, 26 Bromine, reaction with furan in methanol to yield 2,5-dimethoxy-2,5-dihydrofuran, 40, 29
3-Bromoacetophenone, 40, 7
2-Bromoallylamine, 43, 6
2-Bromoallylhexaminium bromide, 43,
6
o-Bromoaniline, conversion to 1-biomo-
2-fluorobenzene, 43, 12
108
SUBJECT INDEX
0-Bromoaniline, diazotization and conversion to o-bromoiodobenzene,
40, 105
in formation of triphenylene via benzyne, 40, 106 9-Bromoanthracene, 43, 16
3-Bromobenzaldehyde, 40, 9 Bromobcnzcne, conversion to Grignard reagent, 41, 91 «-Bromobenzenediazonium hexafluoro-phosphate, 43, 12
3-Bromo-4-ier<-butylacetophenone, 40,
9
BROMOCYCLOPROPANE, 43, 9
1-Bromo-2-iluoeobenzene, 43, 12
l-Bromo-2,5-hexadiene, 41, SI
3-Bromo-l,5-hexadiene, 41, 51 Bromohexadiene (mixture), 41, SO
dehydrobromination to 1,3,5-hexa-triene. 41, 50 isomer mixture of, 41, 51 5-Bromoindo]e-3-carbonitrile, 43,59
0-Bromoiodobenzene, reaction with lithium to form triphenylene, 10, 106
3-Bromo-4-methylacetophenone, 40,9 /’-Bromophenacylamine, hydrochloride of, 41, 87
3-Bromophthalide, 42, 26
3-Bromopropiophenone, 40, 9
1-Bromopyrene, 43,16
2-Bromothiophene, 2-hydroxythiophene from, 43, 55
3-Bromo-4-tolualdehyde, 40, 9 Butadiene, 1-chloro-1,4,4-triflu-
oro-, 43,17
1,3-Butadiene, 1,4-diphenyl-, 40, 36 BlJTADIENOIC ACID, METHYL ESTER, 43, 71
Butenolides from aryl aldehydes and 7-keto acids, 43, 5
2-tert-Butoxythiophene from tert-butyl perbenzoate and 2-thienylmag-nesium bromide, 43, 55 tert-Butyl acetoacetate, 42, 2S sec-Butyl acrylate, 41, 62 sec-Butyl alcohol, esterification of cro-tonic acid with, 41, 60
sec-Butyl alcohol, esters with «,(3-unsat-urated acids, 41, 62 tert-Butyl alcohol, drying with СаНг, 41,
7
oxidation to a,a,a',[/-tetrainethyltet-ramethylene glycol by hydrogen peroxide and ferrous sulfate, 40, 90
reaction with cyanoacetyl chloride, 41, 6
н-Butyl bromide, preparation of к-butyl Grignard reagent from, 41, 61 sec-Butyl cinnamate, 41, 62 sec-Butyl crotonate, 41, 60 reaction with я-butyl Grignard reagent, 41, 61 tert-Butyl cyanoacf.tate, 41, 5 sec-Butyl /3,|3-dimethylacrylate, 41, 62 Butylhydrazinium hydrogen sulfate, 43,
2
tert-Butyl hypochlorite, N-chlormation of amines with, 41, 82 n-Butyl isocyanide, 41,14 iert-Butyl isocyanide, 41,14 я-Butylmagnesium bromide, 41, 61 reaction with sec-butyl crotonate, 41,
61
да-Butyl methacrylate, 41, 62 sec-Butyl 3-methylheptanoate, 41, 61 hydrolysis of, 41, 62 5-Butyl-l, 2,3,4,5-pentachlorocyclo-pentadiene, 43, 92
5-ifx-Buty 1-1,2,3,4,5-pentacblorocyclo-pentadiene, 43, 92 terf-Butyl perbenzoate, 2-<ert-butoxy-thiophene from, 43, 55 reaction with phenylmagnesium bromide, 41, 91 ^-fe^-Butylperoxybenzoic acid, 43, 96 sec-Butyl tiglate, 41, 62
2,3-dimethylheptanoic acid from, 41, 63
2-Butynoic acid, 42, 97
Cadmium chloride as catalyst in conversion of dipotassium 1,8-naph-thalenedicarboxylate to 2,6-naph-thalenedicarboxylic acid, 40, 72
SUBJECT INDEX
109
Calcium hydride, for drying of teri-butyl alcohol, 41, 7 Саевобимше, diphenyl-, 43,31 Carbodiimides, from isocyanates, 43, 31
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