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The diels alder reaction selected practical methods - Fringuelli F.

Fringuelli F. The diels alder reaction selected practical methods - John Wiley & Sons, 2002. - 350 p.
ISBN 0-471-80343
Download (direct link): thedielsalderreaction2002.pdf
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The Diels-Alder Reaction: Selected Practical Methods Edited by Francesco Fringuelli and Aldo Taticchi Copyright 2002 John Wiley & Sons, Ltd ISBNs: 0-471-80343-X (Hardback); 0-470-84581-3 (Electronic)
4 Diels-Alder Reaction Facilitated by Special Physical and Chemical Methods
The Diels-Alder reaction is the most widely used carbon-carbon, carbon-heteroatom and heteroatom-heteroatom bond-forming reaction for the construction of six-membered rings; therefore it is not surprising that many methods have been used to accelerate the reaction and to improve its selectivity. Chapters 2, 3 and 5 illustrate the effects of temperature, Lewis acids and pressure, respectively; this chapter provides a survey of other physical and chemical methods by which the Diels-Alder reaction can be profitably carried out.
A compendium of these special methods was reviewed by Pindur in 1993 [1].
4.1 SOLID-PHASE DIELS-ALDER REACTION
Solid-phase chemistry is an efficient synthetic tool that, compared with solu-tion-phase chemistry, simplifies the work-up of the reaction, allows the process to be driven to completion by using excess of reagents, and can be automatized [2a]. In recent years, many studies have been devoted to developing both surface-mediated and resin-supported synthesis. Today the solid-phase approach is not limited to peptides and oligonucleotides but is also used to synthesize molecules of lower molecular weight.
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