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Chromatographic scince series - Cazes J.

Cazes J. Chromatographic scince series - Marcel Dekker, 1996. - 1098 p.
ISBN 0-8247-9454-0
Download (direct link): сhromatography1996.pdf
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sputtering of sample molecules, 252-258 volatilization of sample molecules, 248-252 Documentation, 35, 226-237 modem techniques, 231-236,237 image processing, 236,237 photocopying, 231 photographing, 231-236 traditional techniques, 229-231 drawing, sketching, or tracing, 230-231
[Documentation] storing the chromatogram, 229-230 Doxycycline, 468-473 Drugs. See Pharmaceuticals and drugs Dyes. See Synthetic dyes
ECTEOLA-cellulose, 925 Efficiency of chromatographic system, measures of, 54-58 models of theoretical plates, 54 selectivity of separation, 58 separation and resolution, 55-58 Van Deemter equation, 54-55 Electron-pair donor/electon-pair acceptor, 4 Enantiomeric mixtures of amino acids and their derivatives, resolution of, 411-419 Enantiomer separations, 621-682 chromatographic methods of configurational analysis, 622 direct separation on TLC plates coated with chiral compounds, 835 with impregnated layers, 122 layers for, 19-20 precoated layers for, 121 separations based on adsorbents with chiral cavities, 622-626 separations on cellulose thin-layer plates, 626-630 separations on microcrystalline triacetylcellulose thin-layer plates, 630-631 separations on polymorphic forms of chitin, 631633
separations using chiral p-cyclodextrin 634-635 separations using diasteromeric derivatives, 635, 647-650
thin-layer enantiomeric resolution via ligand exchange, 651-654 TLC based on silica gel bound to optically active poly(meth)acrylic acid amides, 633-634 TLC based on the molecular imprinting technique, 633
Environmental products, application of TLC to phenolic separations in, 902,903-904 Environmental toxicity, measurement of, 958-959 Enzyme inhibition (pesticide detection system), 806-807 Ergocalciferol (vitamin D2), 1061 Erythromycin, 463-468
Fast atom bombardment (FAB), 837 TLC/MS and, 34, 243,245, 247, 253, 254, 256, 259
Fiber dyes, 1005
Index
1095
Flame ionization detectors (FID), 171,361-372 applications of TLC-FID systems, 369 coated rod systems, 366-369 tubular systems, 365 TLC-FID systems, 362-369 coated rod systems, 364-369 tubular systems, 362-364 Flame thermionic ionization detector (FTID), 369 Flat-bed chromatography, 3 Flavonoids, 717-722 distribution, 717 practical experiments, 719-722 structure, 717 TLC of, 718-719 Fluorescence, 939 measurement of, 208-210 for quantitative determination in TLC, 281-287 Fluorgenic detection (pesticide detection system), 810-811 Folic acid, 1051 Food additives, 803 Food dyes, 1006-1014 Foodstuff dyes, 1004
Forced flow planar chromatography (FFPC), 2930, 307, 826 Fourier-transform (FT), 33 Fourier-transform infrared (FTIR) spectroscopy, 221-222, 224, 225, 940 evaluation of thin-layer chromatogram, 147 Fruit material, sample preparation of, 484 Fungicides:
extraction and cleanup procedures for, 754, 755759
TLC procedures for, 785-788 Fungitests, 807-810
Gangliosides, 694,696
Gas chromatography/mass spectrometry (GC/MS), 243
Gas chromatography/TLC (GC/TLC), 940 Gentamicin, 457-458 Glossary, 1079-1086 Glycolipids: for lipid extractions, 691 one-dimensional solvent systems for TLC of,
693-694
two-dimensional solvent systems for TLC of, 695-696 Gossypol, 1042-1043 Gradient development, 30-31,149-170 apparatus for, 151-154 devices for achieving mobile-phase gradient, 151-153
[Gradient development]
devices for achieving stationary-phase gradients, 153-154 classification of gradients according to shape, 150-151 gradient elution, 154-161 automated multiple development, 160-161 mobile-phase gradient, 156-157 optimization strategy in gradient elution, 157 159
polyzonal TLC, 154-156 stationary-phase gradient, 159-160 gradient elution in analytical and preparative TLC, 166 history, 150 nomenclature, 150
optimization of stepwise gradient elution, 162 166
graphical method, 162-163 numerical method, 163-166 Griseofulvin 474-476
Growth regulators. See Herbicides and growth regulators
Herbicides and growth regulators, 774785 chlorophenoxyalkylcarboxylic acid herbicides, 781-783 diphenyl ether herbicides, 779-781 extraction and cleanup procedures for, 754, 755759
growth regulators, 784-785 thiocarbamates, 784 triazines. 774-779 Highly polar steroids, separation of, 974 High-performance liquid chromatography (HPLC),
171
of antibiotics, 446
differences between TLC and, 131, 923 direct sampling of TLC and, 146-147 OPLC as pilot technique for, 191 retention transfer between TLC and, 177-178 transfer of results from TLC to, 40 High-performance thin-layer chromatography (HPTLC), 5, 78-79, 172, 307, 753, 877 of antibiotics, 445-446 comparison of TLC to, 5-6 of dyes, 1024-1026 separation of amino acids by, 406-411 High-speed thin-layer chromatography (HSTLC),
172
History of TLC, 4-5
Hydroazinolysis, alteration of nucleic acids by, 946 Hydrogen bonding, 4
1096
Index
Hydrophilic vitamins, 1047-1054 ascorbic acid (vitamin C), 1052-1053 biotin, 1051-1052
cobalanin (vitamin B12), 1049-1050, 1051, 1052 folic acid, 1051
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